The alkyne complexes [Mo2(µ-C2Ph2)(CO)4(η-C5H5)2] and [Co2(µ-C2Ph2)(CO)6] reacted together to give the butterfly cluster [Co2Mo2(µ3-CPh)2(µ4-C2Ph2)(CO)4(η-C5H5)2], which can also be made from [Mo2(µ-C4Ph4)(CO)(η-C5H5)2] and [Co2(CO)8]; the possible role of the C4Ph4 complex as an intermediate in the former transformation is discussed.
H. Adams, L. J. Gill and M. J. Morris, J. Chem. Soc., Dalton Trans., 1996, 3909 DOI: 10.1039/DT9960003909
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