Reaction of ethyl bromoacetate and zinc with [60]fullerene in the absence of any solvent, followed by quenching with acid affords 1-ethoxycarbonylmethyl-1-20 dihydro [60]fullerene along with other minor byproducts including 1,4-bis(ethoxycarbonylmethyl)-1,4-dihydro[60]fullerene; a detailed reaction mechanism is proposed.
G. Wang, Y. Murata, K. Komatsu and T. S. M. Wan, Chem. Commun., 1996, 2059 DOI: 10.1039/CC9960002059
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