Acenaphthenone (ANO) is an effective electron donor and undergoes stepwise photooxygenation sensitized by 9,10-dicyanoanthracene, affording hydroxylactone and anhydride derivatives; the electron transfer mechanism via an enol intermediacy was verified by the enhancement effect of biphenyl, fluorescence quenching, exciplex emission and chemically induced dynamic nuclear polarization (CIDNP).
S. Wu, J. Liu and Z. Jiang, Chem. Commun., 1996, 493 DOI: 10.1039/CC9960000493
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