An unprecedented singly deprotonated macrocyclic dioxotetraamine copper(II) complex is prepared and characterized by IR, UV–VIS, EPR and X-ray crystallography; it is established that the enolic tautomer of the amide is present; two double deprotonated copper(II) complexes are prepared for comparison.
F. Kou, S. Zhu, H. Lin, Y. Chen, H. Wang and X. Yao, Chem. Commun., 1996, 59 DOI: 10.1039/CC9960000059
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