Appropriate nitrate esters are cleaved under photolytic or thermal (tributyltin radical) conditions to yield dioxolanyl radicals which undergo stereoselective cyclisation to heterocyclic products. The X-ray crystallographic structures for compounds 30a and 35 are reported.
A. S. Batsanov, M. J. Begley, R. J. Fletcher, J. A. Murphy and M. S. Sherburn, J. Chem. Soc., Perkin Trans. 1, 1995, 1281 DOI: 10.1039/P19950001281
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