Perfluoroalkylated heterocyclic phosphonates have been conveniently synthesized by 1,3-dipolar cyclo-addition of aromatic nitrile oxides (or ethyl diazoacetate or tert-butyl azidoacetate) and perfluoroalkylated alkynylphosphonates in good to excellent yields with high regioselectivity.
Y. Shen, J. Zheng, Y. Xin, Y. Lin and M. Qi, J. Chem. Soc., Perkin Trans. 1, 1995, 997 DOI: 10.1039/P19950000997
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