27 Al NMR measurements in the liquid and the solid state supplemented with chemical analysis of the mixed salts unambiguously reveal that neither tetrahedral nor octahedral aluminium can be substituted by either iron or chromium in Al13-Keggin ion salts prepared by conventional methods.
J. B. Nagy, J. Bertrand, I. Palinkó and I. Kiricsi, J. Chem. Soc., Chem. Commun., 1995, 2269 DOI: 10.1039/C39950002269
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