2-Diphenylphosphinoyl-N,N-dimethylaniline is oxidized at nitrogen by a dilute solution of H2O2 in the presence of MoO(O2)2·(H2O)x; the resulting phosphorus–nitrogen dioxo-ligand forms a molybdenum oxobisperoxo complex, which is structurally characterized by single crystal X-ray diffraction.
W. R. Thiel, T. Priermeier and T. Bog, J. Chem. Soc., Chem. Commun., 1995, 1871 DOI: 10.1039/C39950001871
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