Stable isotope incorporation experiments with 13C- and 18O-labelled precursors show that all the carbon atoms in DTX-4 2 and an okadaic acid diol ester 3 are derived from acetate and glycolate, and also identify the acetate and glycolate derived oxygen atoms.
J. Needham, T. Hu, J. L. McLachlan, J. A. Walter and J. L. C. Wright, J. Chem. Soc., Chem. Commun., 1995, 1623 DOI: 10.1039/C39950001623
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