The carbohydrate-derived α-bromo ketones 4 and 5undergo reductive cleavage using either Zn–Cu or CeCl3–Nal and the resulting enolates are trapped by carbohydrate-based aldehydes 6, 7 and 14 to give C-disaccharide derivatives.
H. M. Binch, A. M. Griffin, S. Schwidetzky, M. V. J. Ramsay, T. Gallagher and F. W. Lichtenthaler, J. Chem. Soc., Chem. Commun., 1995, 967 DOI: 10.1039/C39950000967
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