Cyclic sulfates of vic-diols are transformed in one-pot into sugar episulfides by treatment with potassium thioacetate or thiourea followed by reaction with sodium methoxide; reaction of these cyclic sulfates with potassium selenocyanate followed by treatment with sodium borohydride allows the synthesis of sugar olefins.
F. Santoyo-González, F. García-Calvo-Flores, P. García-Mendoza, F. Hernandez-Mateo, J. Isac-García and M. xmlns="http://www.rsc.org/schema/rscart38"> <. D. Pérez-Alvarez, J. Chem. Soc., Chem. Commun., 1995, 461 DOI: 10.1039/C39950000461
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