It is demonstrated herein that a combination of high-power proton decoupling and magic angle spining can give acceptable high-resolution 19F NMR spectra of simple solid multi-fluorinated organic molecules, as exemplified by three fluorosteroids.
S. A. Carss, R. K. Harris, P. Holstein, B. J. Say and R. A. Fletton, J. Chem. Soc., Chem. Commun., 1994, 2407 DOI: 10.1039/C39940002407
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