Single crystals of pseudopolymorphic modifications [Ph4C6(C)2˙–Na+(OC5H10)n]∞ grow from tetrahydron solution (n= 2, orthorhombic, Pcca, Z= 4) or after equimolar addition of tetramethylendiamine (n= 3, monoclinic, P21/c, Z= 4) and provide information on subtle changes within the same structural motif in accord with the principle of dense lattice packing.
H. Bock, A. John and C. Näther, J. Chem. Soc., Chem. Commun., 1994, 1939 DOI: 10.1039/C39940001939
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