In dichloromethane solution at room temperature, the reaction between [Re4H4(CO)12] and acetone followed by addition of NEt4BF4 Yielded [NEt4]+2[Re3H2(CO)9BF4]2–(30% yield), in which the triangular trirhenium cluster is capped by a µ-FBF3–.
C. S. Yang, H. C. Horng, F. L. Liao and C. P. Cheng, J. Chem. Soc., Chem. Commun., 1994, 1637 DOI: 10.1039/C39940001637
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