Isoprene reacts with aldehydes in the presence of a catalytic amount of Pd(OAc)2–4PPh3 or Pd(PPh3)4 and a stoichiometric amount of SnCl2 at 40–50 °C in AcOH–H2O to produce 1-substituted 2,2-dimethyl-3-buten-1-ols regioselectively.
Y. Masuyama, M. Tsunoda and Y. Kurusu, J. Chem. Soc., Chem. Commun., 1994, 1451 DOI: 10.1039/C39940001451
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