α,β-Unsaturated nitroalkenes were synthesized in 54–99% yields by sonication of a chloroform solution containing the corresponding alkenes, NaNO2(10 equiv.), Ce(NH4)2(NO3)6(2.0 equiv.), and acetic acid (12 equiv.) in a sealed tube at 25–73 °C.
J. R. Hwu, K. Chen and S. Ananthan, J. Chem. Soc., Chem. Commun., 1994, 1425 DOI: 10.1039/C39940001425
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