A rapid method is reported for the hydrothermal synthesis of AlPO4-5 by which the 100% pure crystalline phase is obtained in 90 min at 150 °C using aluminium triisopropoxide, phosphoric acid and tripropylamine in the system free of F– ions.
B. L. Newalkar, R. V. Jasra, V. Kamath and T. S. G. Bhat, J. Chem. Soc., Chem. Commun., 1994, 1041 DOI: 10.1039/C39940001041
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