Methyl 2-hydroxy-α-D-pyranosides were formed via photolytic radical substitution of methyl 2-deoxy-2-iodo-α-D-pyranosides with 2,2,6,6-tetramethylpiperidinoxy (TEMPO) free radical followed by zinc reduction.
A. G. M. Barrett and D. J. Rys, J. Chem. Soc., Chem. Commun., 1994, 837 DOI: 10.1039/C39940000837
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