Oxygen-17 magic angle spinning NMR spectroscopy of TiO2–SiO2 gels formed by hydrolysis of alkoxides with 17O-labelled water provides a novel technique for detecting amorphous or poorly crystalline impurity phases and atomic scale phase separation.
M. E. Smith and H. J. Whitfield, J. Chem. Soc., Chem. Commun., 1994, 723 DOI: 10.1039/C39940000723
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