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The first free-radical synthesis of isocyanates was performed by oxidation of oxalic acid monoamides by S2O82–, catalysed by silver(I) and copper(II) salts, in a two-phase system.
F. Minisci, F. Coppa and F. Fontana, J. Chem. Soc., Chem. Commun., 1994, 679 DOI: 10.1039/C39940000679
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