A simple route to layered tetravalent metal phosphonates containing amide linkages is demonstrated by a model reaction in which the ethylenediammonium ion exchanged form of layered zirconium carboxyethyl-phosphonate is converted into the amide derivative by thermal condensation.
T. Kijima, Y. Kawagoe, K. Mihara and M. Machida, J. Chem. Soc., Dalton Trans., 1993, 3827 DOI: 10.1039/DT9930003827
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