Issue 23, 1993
From the journal:

Journal of the Chemical Society, Dalton Transactions

Preparation and crystal structure of a seven-co-ordinated oxotungsten(IV) complex of 2,2′:6′,2″:6″,2‴-quaterpyridine

San-Ming Yang,   Kung-Kai Cheung  and  Chi-Ming Che  

Abstract

The reaction of [WOCl2(PMe2Ph)3] with 2,2′:6′,2″:6″,2‴-quaterpyridine (L) in ethanol gave [WO(PMe2Ph)2L]2+ isolated as a BPh4– salt. X-Ray diffraction analysis revealed that the complex cation adopts a distorted pentagonal-bipyramidal structure with the W[triple bond, length as m-dash]O distance being 1.696(9)Å. The spectroscopic properties and electrochemistry of this tungsten complex have been investigated.

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Article information

DOI
https://doi.org/10.1039/DT9930003515
Article type
Paper

J. Chem. Soc., Dalton Trans., 1993, 3515-3517

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Preparation and crystal structure of a seven-co-ordinated oxotungsten(IV) complex of 2,2′:6′,2″:6″,2‴-quaterpyridine

S. Yang, K. Cheung and C. Che, J. Chem. Soc., Dalton Trans., 1993, 3515 DOI: 10.1039/DT9930003515

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