Products from the reaction of MCl5(M = Nb or Ta) with acids RCO2H (R = aryl) include the tetranuclear tantalum oxo cluster [{TaCl2(µ-O)(O2CC6H4Me-p)}4] containing a Ta4O4 core, dinuclear [{NbCl3-(O2CR)}2(µ-O)], and the monosubstituted [TaCl4(O2CR)].
D. A. Brown, W. Errington and M. G. H. Wallbridge, J. Chem. Soc., Dalton Trans., 1993, 1163 DOI: 10.1039/DT9930001163
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