The phosphorus coordination of the diphenyl(dithioformato)phosphine ligand in [W(CO)5(PPh2CS2)]Et4N, 1has been confirmed by an X-ray diffraction analysis; alkylation of 1 at the S atom results in the formation of W(CO)5[PPh2(CS2R)], 4in high yield.
K. Yih, Y. Lin, M. Cheng and Y. Wang, J. Chem. Soc., Chem. Commun., 1993, 1380 DOI: 10.1039/C39930001380
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