High resolution powder X-ray diffraction using synchrotron radiation has established the formulation [PCl4+]2[PCl6–][Cl–] for a metastable form of PCl5 with significant interaction between the PCl4+ and Cl– ions.
A. Finch, A. N. Fitch and P. N. Gates, J. Chem. Soc., Chem. Commun., 1993, 957 DOI: 10.1039/C39930000957
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