NH2(CH2)3Si(OC2H5)3 has been exchanged into layered niobate KNb3O8to form an intercalate with an interlayerdistance of 26.8 Å, calcination of this intercalate in O2 at 600 °C gives rise to the first porous silica-pillared layered niobate with a Brunauer-Emmett-Teller (BET) surface area of 165 m2g–1.
W. Hou, B. Peng, Q. Van, X. Fu and G. Shi, J. Chem. Soc., Chem. Commun., 1993, 253 DOI: 10.1039/C39930000253
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