The preparation of TlITCNQ and its 18-crown-6 complex are reported together with an X-ray structural study of the latter which provides the first example of a crown ether-complexed Tl+ salt in which the lone pair plays an active stereochemical role in the solid state.
M. C. Grossel and S. C. Weston, J. Chem. Soc., Chem. Commun., 1992, 1510 DOI: 10.1039/C39920001510
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