The reaction of LiP(CH2CH2PMe2)2 with ThCl4 gives rise to the first actinide tetraphosphido complex, Th[P(CH2CH2PMe2)2]4; the first member of a class of f-element complexes bonded solely to phosphorous ligands and for which spectroscopic, analytical and X-ray crystallographic characterisation is presented.
P. G. Edwards, M. Harman, M. B. Hursthouse and J. S. Parry, J. Chem. Soc., Chem. Commun., 1992, 1469 DOI: 10.1039/C39920001469
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