The nickel-catalysed cross-coupling reactions of tetrathioorthocarbonate 1 with Grignard reagents give the corresponding substituted alkenes in moderate to good yields; this reaction demonstrates the first example of using tetrathioorthocarbonate as a C4+ synthon.
W. Cheng and T. Luh, J. Chem. Soc., Chem. Commun., 1992, 1392 DOI: 10.1039/C39920001392
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