A new synthesis and crystal structure of 2-methyl-2-azabicyclo[3.3.1]nonan-7α-ol
Abstract
A facile, high yield synthesis of 2-methyl-2-azabicyclo[3.3.1]nonan-7α-ol 2b from cyclohex-3-ene-1-carbaldehyde 3 is reported; an X-ray structure of 2b·HCl established the stereochemical assignment of 2b.