Reaction of PdCl2(PPh3)21 with an excess of H2SiMePh and 2,6-xylyl isocyanide gives [graphic omitted]R)C(![[double bond, length half m-dash]](https://www.rsc.org/images/entities/char_e006.gif)
NR)CH(NR)}(C![[triple bond, length half m-dash]](https://www.rsc.org/images/entities/char_e007.gif)
NR)Cl·1/2C6H6(3, R = 2,6-xylyl) and heterobicyclic compound, 2,6-(2′,6′-xylyl)2-3,7-(N-2′,6′-xylylimino)2-4,8-(N-2′,6′-xylylamino)2-2,6-diaza-bicyclo[3.3.0]octa-4,8-diene 4; the structures of which have been determined by X-ray analysis.
T. Tanase, T. Ohizumi, K. Kobayashi and Y. Yamamoto, J. Chem. Soc., Chem. Commun., 1992, 707 DOI: 10.1039/C39920000707
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