Upon treatment with mercury(II) acetate and perchloric acid catalyst, hemiperoxyacetals derived from 1-phenlprop-2-enyl hydroperoxide afford 3,5,6-trisubstituted 1,2,4-trioxanes with high diastereoselectivity whereas those derived from 3-phenylprop-2-enyl hydroperoxide yield only 3-phenyl-4-mercurio-1,2-dioxolane.
A. J. Booldworth and N. A. Tallant, J. Chem. Soc., Chem. Commun., 1992, 428 DOI: 10.1039/C39920000428
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