Bis(3,5-di-tert-butylcatecholato)(phenanthroline)vanadium(IV)1 is prepared, and oxidised with silver hexafluorentimonate to give its vanadium(V) analogue 2; both complexes are characterised by X-ray crystallography revealing significant differences in their coordination geometry.
T. A. Kabanos, A. J. P. White, D. J. Williams and J. D. Woollins, J. Chem. Soc., Chem. Commun., 1992, 17 DOI: 10.1039/C39920000017
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