An HNO3—HClO4 dissolution procedure followed by evaporation, re-dissolution and dilution with a CH3CO2H—KNO3 electrolyte is shown to be effective for the treatment of soil samples prior to the determination of trace amounts of lead by differential-pulse anodic stripping voltammetry.
A. R. Fernando and J. A. Plambeck, Analyst, 1992, 117, 39 DOI: 10.1039/AN9921700039
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