Total reflection X-ray fluorescence spectrometry (TXRF) has been shown to be applicable when determining different oxidation states in a variety of compounds by the method of Kβ/Kα intensity ratioing. It has also been shown that by using TXRF it is possible to relate shifts in the intensity ratio to coordination bonding.
S. Mukhtar and S. J. Haswell, J. Anal. At. Spectrom., 1991, 6, 339 DOI: 10.1039/JA9910600339
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