By γ-irradiation of the completely deuteriated compounds, (C6D5)nSiD3-n(where n= 1–3), at 77 K, the anisotropic 29Si couplings in the corresponding radicals, (C6D5)nSiD3-n, have been measured for the first time.
W. Lim and C. J. Rhodes, J. Chem. Soc., Chem. Commun., 1991, 1228 DOI: 10.1039/C39910001228
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