Photolysis of benzofurazan 1-oxide 3 and 2-nitrophenyl azide 7 in Ar matrices at 14 K yielded 1,2-dinitrosobenzene 4, which had not previously been characterized; the IR and UV absorptions of matrix-isolated 4 have been recorded, and its, thermal and photochemical reversion to 3 has also been observed, 15N labelling experiments lend strong support to the assignment.
I. R. Dunkin, M. A. Lynch, A. J. Boulton and N. Henderson, J. Chem. Soc., Chem. Commun., 1991, 1178 DOI: 10.1039/C39910001178
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