The reaction of [VO(salen)] with controlled quantities of species able to extract the oxygen atom, such as trityl fluoroborate or fluoroboric acid–diethyl ether (1/1) leads to the novel tetranuclear cation [{V(salen)}4(µ-O)3]2+, which contains a linear vanadium–oxygen chain.
A. Hills, D. L. Hughes, G. J. Leigh and J. R. Sanders, J. Chem. Soc., Chem. Commun., 1991, 827 DOI: 10.1039/C39910000827
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