Treatment of cobalt(II) porphyrins with hydroperoxides and an excess of NaBH4 effectively gave σ-alkylcobalt(III) porphyrins, the σ-alkyl groups of which were derived from ethers used as solvents.
J. Setsune, Y. Ishimaru, T. Moriyama and T. Kitao, J. Chem. Soc., Chem. Commun., 1991, 556 DOI: 10.1039/C39910000556
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