The electrosynthesis of 2-vinylidene-3-yne carboxylic acids from carbon dioxide and substituted 1,3-diynes is catalysed by a nickel–triamine complex and results in a regio- and stereo-selective addition to one triple bond.
S. Dérien, J. Clinet, E. Duñach and J. Périchon, J. Chem. Soc., Chem. Commun., 1991, 549 DOI: 10.1039/C39910000549
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