Tetrathiafulvalenes such as bis(ethylenedithio)tetrathiafulvalene (BEDT-TTF) having alkylthio substituents have been prepared in good yields by direct desulphurization of 1,3-dithiole-2-thiones with trimethyl phosphite under high pressure.
Y. Yamashita, M. Tomura and S. Tanaka, J. Chem. Soc., Perkin Trans. 1, 1990, 3358 DOI: 10.1039/P19900003358
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