26,27-Dinorbrassinolide, having a (20S,22R,23R)-22,23-dihydroxy-unit side-chain, was stereo-selectively synthesized from hyodeoxycholic acid via successive lactonization, oxidation, and reduction of the key intermediate (Z)-(7).
Z. Wei-Shan, Z. Hui-Qiang and W. Zhi-Qin, J. Chem. Soc., Perkin Trans. 1, 1990, 2281 DOI: 10.1039/P19900002281
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