A new method for the stereocontrolled synthesis of 2,3,3-trisubstituted cyclohexanones is reported which involves the first example of hydroxylactonisation of a γ,δ-unsaturated tertiary amide followed by reductive cleavage of the lactone to produce the substituted cyclohexanone.
P. M. Cairns, C. Howes and P. R. Jenkins, J. Chem. Soc., Perkin Trans. 1, 1990, 627 DOI: 10.1039/P19900000627
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