A simple synthesis of tritiated or deuteriated methylene diiodide is reported, providing a useful reagent for the incorporation of tritium or deuterium into a cyclopropyl ring through the Simmons–Smith reaction, as illustrated by regiospecific addition to perillyl alcohol.
M. Saljoughian, H. Morimoto, P. G. Williams and N. DeMello, J. Chem. Soc., Chem. Commun., 1990, 1652 DOI: 10.1039/C39900001652
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