The oxidative cyclisation of 5-stannyl-1,3-pentanediol derivatives gave corresponding 4-hydroxytetrahydropyrans in excellent yields, and its applications to the synthesis of dioxabicyclodecane 12 and 4-hydroxy-δ-lactone 14 are also described.
M. Yamamoto, S. Irie, T. Arase, S. Kohmoto and K. Yamada, J. Chem. Soc., Chem. Commun., 1990, 1492 DOI: 10.1039/C39900001492
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