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The 27Al quadrupolar coupling parameters (CQ= 3.90 MHz and η= 0.30) and a high content of metallic aluminium (16 ± 2 atom %) have been determined for commercial LiAlH4 using 27Al MAS NMR spectroscopy.
L. Kellberg, H. Bildsøe and H. J. Jakobsen, J. Chem. Soc., Chem. Commun., 1990, 1294 DOI: 10.1039/C39900001294
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