SCHEDULED MAINTENANCE
Protected glucopyranosylidene diazides have been obtained in good yields by two routes which involve nucleophilic substitutions at the anomeric polsition of either 2,3,4,6-tetra-O-acetyl-1-bromo-β-D-glucopyranosyl chloride or 2,3,4,6-tetra-O-benzyl-D-glucono-1,5-lactone, in the presence of silver azide or trimethylsilyl azide, respectively.
J.-P. Praly, Z. E. Kharraf and G. Descotes, J. Chem. Soc., Chem. Commun., 1990, 431 DOI: 10.1039/C39900000431
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