The cluster [Os4(CO)12(C9H6)](1) has been isolated from the reaction of [Os3(CO)12] with indene in nonane under reflux; X-ray analysis has shown that (1) has a ‘butterfly’ metal framework while the indyne group interacts with the metal atoms via two σ-bonds and two π-bonds.
H. Chen, B. F. G. Johnson, J. Lewis and P. R. Raithby, J. Chem. Soc., Chem. Commun., 1990, 373 DOI: 10.1039/C39900000373
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