The interference-free generation of AsH3 in the presence of 800 mg l–1 of selenium is described. The dissolved selenium is reduced to the elemental state with hydrazine and the precipitate is allowed to settle, but is not removed from the flask before the hydride generation.
R. Bye and W. Lund, J. Anal. At. Spectrom., 1989, 4, 233 DOI: 10.1039/JA9890400233
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