A rhodium(III) complex in N,N-dimethylacetamide solution under a 1 atm O2/H2 mixture catalyses concomitant formation of the hydroperoxide MeC(O)N(Me)CH2OOH and hydrogen peroxide.
S. N. Gamage and B. R. James, J. Chem. Soc., Chem. Commun., 1989, 1624 DOI: 10.1039/C39890001624
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